| Analysis |
Method |
Water/Liquid |
Soil/Sludge* |
| Container |
Quantity |
Preservative (All samples at 4 C) |
Holding Time |
Holding Time |
| Volatiles |
| TPH (TX 1005) |
TX 1005 |
VOA |
2 vials |
NaHSO4 |
14 d |
14 d |
| TPH (TX 1006) |
TX 1006 |
VOA |
2 vials |
NaHSO4 |
14 d |
14 d |
| BTEX |
8021 |
VOA |
2 vials |
HCl |
14 d |
14 d |
| BTEX/MTBE |
8021 |
VOA |
2 vials |
HCl |
14 d |
14 d |
| BTEX/MTBE |
8260 |
VOA |
2 vials |
HCl |
14 d |
14 d |
| GRO (gasoline) |
8015M |
VOA |
2 vials |
HCl |
14 d |
14 d |
| VOCs by GC/MS |
524, 624, 8260 |
VOA |
2 vials |
HCl |
14 d |
14 d |
| Alcohols |
8015M |
VOA |
2 vials |
|
14 d |
14 d |
| Semi-Volatiles |
| DRO/ORO (Diesel or oil) |
8015M |
AG |
1 Liter |
|
7 d |
14 d |
| Herbicides |
8151 |
AG |
1 Liter |
|
7 d |
14 d |
| PCBs |
8082, 608 |
AG |
1 Liter |
|
7 d |
14 d |
| Pesticides |
8081, 608 |
AG |
1 Liter |
|
7 d |
14 d |
| Pesticides & PCBs |
8081/8082, 608 |
AG |
1 Liter |
|
7 d |
14 d |
| Phenolic Compounds |
625, 8270 |
AG |
1 Liter |
|
7 d |
14 d |
| Organo-Phos Pesticides |
8141 |
AG |
1 Liter |
|
7 d |
14 d |
| PAHs |
8310, 8270 |
AG |
1 Liter |
|
7 d |
14 d |
| SVOC by GC/MS |
625, 8270 |
AG |
1 Liter |
|
7 d |
14 d |
| Glycols |
8015M |
AG |
1 Liter |
|
7 d |
14 d |
| Metals |
| Individual Metals |
200, 6000, 7000 |
poly |
500 mL |
HNO3 |
6 mth |
6 mth |
| Chromium VI |
7196 |
poly |
500 mL |
|
24 h |
28 d |
| Mercury |
245.1, 7470/7471 |
poly |
500 mL |
HNO3 |
24 d |
28 d |
| TCLP/SPLP |
| TCLP/SPLP Volatile |
1311/1312/8260 |
VOA |
100 mL |
|
7 d |
14 d |
| TCLP/SPLP Semi-volatile |
1311/1312/8270 |
AG |
1 Liter |
|
7 d |
14 d |
| TCLP/SPLP Pesticides |
1311/1312/8081 |
AG |
1 Liter |
|
7 d |
14 d |
| TCLP/SPLP Herbicides |
1311/1312/8151 |
AG |
1 Liter |
|
7 d |
14 d |
| TCLP/SPLP Metals |
1311/1312/6010/7470 |
poly or glass |
500 mL |
|
28 d |
28 d |
|
|
|
|
|
|
|
| *Soil Sludge can be collected in 4 oz. or 8 oz glass jars with Teflon lid and preserved at 4C |
|
  |
| Analysis |
Method |
Water/Liquid |
Soil/Sludge* |
| Container |
Quantity |
Preservative (All samples at 4 C) |
Holding Time |
Container |
Holding Time |
| Inorganics/Wet Chemistry |
| Acidity |
305.1 |
poly or glass |
100 mL |
|
14 d |
4 oz Glass |
14 d |
| Alkalinity |
310.1 |
poly or glass |
100 mL |
|
14 d |
4 oz Glass |
14 d |
| Ammonia |
350.3 |
poly or glass |
500 mL |
H2SO4 |
28 d |
4 oz Glass |
28 d |
| BOD |
405.1 |
poly |
1 Liter |
|
48 h |
…… |
…… |
| Bromide |
300 |
poly or glass |
100 mL |
|
28 d |
4 oz Glass |
28 d |
| Chloride |
325.3 |
poly or glass |
100 mL |
|
28 d |
4 oz Glass |
28 d |
| Chlorine |
330.3 |
poly or glass |
200 mL |
|
imm. |
…… |
…… |
| COD |
410.4 |
poly or glass |
50 mL |
H2SO4 |
28 d |
…… |
…… |
| Coliform |
Hach 8368 |
poly or glass |
100 mL |
Na2S2O3 |
imm. |
4 oz Glass |
imm. |
| Color |
110.2 |
poly or glass |
500 mL |
|
48 h |
…… |
…… |
| Cyanide (Reactive) |
SW 7.3.3.2 |
poly or glass |
500 mL |
|
14 d |
4 oz Glass |
14 d |
| Cyanide (Total) |
335.2 |
poly or glass |
500 mL |
NaOH |
14 d |
4 oz Glass |
14 d |
| Dissolved Oxygen |
360.1 |
poly or glass |
100 mL |
|
imm. |
…… |
…… |
| Flashpoint |
1010/1030 |
glass |
100 mL |
|
N/A |
4 oz Glass |
N/A |
| Fluoride |
340.2 |
poly or glass |
500 mL |
|
28 d |
4 oz Glass |
28 d |
| Hardness |
130.2/6010 |
poly or glass |
500 mL |
HNO3 |
6 mth |
…… |
…… |
| Ignitability |
1010 |
glass |
100 mL |
|
N/A |
4 oz Glass |
N/A |
| MBAS (Surf.) |
425.1 |
poly or glass |
1 Liter |
|
48 h |
…… |
|
| Nitrate-Nitrite |
353.3 |
poly or glass |
500 mL |
H2SO4 |
28 d |
4 oz Glass |
28 d |
| Odor |
140.1 |
AG |
500 mL |
|
24 h |
…… |
…… |
| Oil and Grease |
413.1 |
AG |
1 Liter |
H2SO4 |
28 d |
…… |
…… |
| Paint Filter |
9095 |
poly or glass |
…… |
…… |
…… |
4 oz Glass |
N/A |
| pH |
150.1, 9045 |
poly or glass |
100 mL |
none |
imm. |
4 oz Glass |
imm. |
| Phenols (Total) |
420.1 |
A VOA |
40mL |
H2SO4 |
28 d |
4 oz Glass |
28 d |
| Phosphate |
365.2 |
AG |
100 mL |
|
48 h |
4 oz Glass |
48 h |
| Phosphorus |
365.2 |
poly or glass |
100 mL |
H2SO4 |
28 d |
4 oz Glass |
28 d |
| Settleable Solids |
160.5 |
poly or glass |
1 Liter |
|
imm. |
…… |
…… |
| Spec. Conductance |
120.1 |
AG |
500 mL |
|
48 h |
4 oz Glass |
28 d |
| Sulfate |
9038/375.4 |
poly or glass |
500 mL |
|
28 d |
4 oz Glass |
28 d |
| Sulfide |
9030/376.1 |
poly or glass |
500 mL |
NaOH + Zn |
7 d |
4 oz Glass |
7 d |
| Sulfide, Reactive |
SW 7.3.4.2 |
poly or glass |
500 mL |
|
7 d |
4 oz Glass |
7 d |
| Sulfite |
377.1 |
poly or glass |
100 mL |
|
imm. |
4 oz Glass |
imm. |
| TDS |
160.1 |
poly or glass |
500 mL |
|
7 d |
…… |
…… |
| TKN |
351.4 |
poly or glass |
500 mL |
H2SO4 |
28 d |
4 oz Glass |
28 d |
| TOC |
415.1, 9060 |
VOA |
2 vials |
HCl |
28 d |
4 oz Glass |
28 d |
| TOX |
9020 |
AG |
500 mL |
|
28 d |
4 oz Glass |
28 d |
| Total Solids |
160.3 |
poly or glass |
500 mL |
|
7 d |
4 oz Glass |
7 d |
| TSS |
160.2 |
poly or glass |
500 mL |
|
7 d |
…… |
…… |
| Turbidity |
180.1 |
poly or glass |
100 mL |
|
48 h. |
…… |
…… |
| TVS (vol. solids) |
160.4 |
poly or glass |
500 mL |
|
7 d |
…… |
…… |
|
